Derivatization of Corn Oil for Analysis by GC | LabRulez GCMS
 

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Application Note123Derivatization of Corn Oil for Analysis by GCHIn the derivatization of corn oil fatty acids with methanolicHCl, a general purpose transesterification reagent, removal of one of the reaction products drives the reactiontoward completion. 2,2-Dimethoxypropane increases themethyl ester yield by...
Klíčová slova
fatty, fattytransesterification, transesterificationglycerol, glycerolhcl, hclmethanolic, methanolicchoh, chohesters, estersreaction, reactioncorn, cornacid, acidextra, extramethyl, methylbyproducts, byproductsincomplete, incompletedmso
TheReporterReprinted from Volume 16, No. 3, 1997T297053© 1999 Sigma-Aldrich Co.For more information, or current prices, contact your nearest Supelco subsidiary listed below. To obtain further contact information, visit our website (www.sigma-aldrich.com), see the Supelco catalog, orcontact Supelco, Bellefonte, PA 16823-0048...
Klíčová slova
transesterification, transesterificationglycerol, glycerolhcl, hcllipid, lipidesters, esterscorn, cornreaction, reactionmethanolic, methanolictriglyceride, triglyceridefatty, fattybyproducts, byproductsdmso, dmsoacid, acidoil, oilexcess
Bulletin 909AGuide to Derivatization Reagents for GCA large number of reagents are used to prepare derivatives forgas chromatography, but most of the derivatization reactionsfit into one of three categories: acylation, alkylation, orsilylation. This bulletin describes each category, and presentsinformation on...
Klíčová slova
trimethylsilyl, trimethylsilylethers, etherstmcs, tmcstmsi, tmsibstfa, bstfaalkylation, alkylationsilylation, silylationhmds, hmdsesters, estersacylation, acylationdmf, dmfsupelco, supelcobsa, bsadialkylacetals, dialkylacetalsreagents
Bulletin 909AGuide to Derivatization Reagents for GCA large number of reagents are used to prepare derivatives forgas chromatography, but most of the derivatization reactionsfit into one of three categories: acylation, alkylation, orsilylation. This bulletin describes each category, and presentsinformation on...
Klíčová slova
trimethylsilyl, trimethylsilylethers, etherstmcs, tmcstmsi, tmsibstfa, bstfaalkylation, alkylationsilylation, silylationhmds, hmdsesters, estersacylation, acylationdmf, dmfsupelco, supelcobsa, bsadialkylacetals, dialkylacetalsreagents
 

Podobná PDF

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Application Note123Derivatization of Corn Oil for Analysis by GCHIn the derivatization of corn oil fatty acids with methanolicHCl, a general purpose transesterification reagent, removal of one of the reaction products drives the reactiontoward completion. 2,2-Dimethoxypropane increases themethyl ester yield by...
Klíčová slova
fatty, fattytransesterification, transesterificationglycerol, glycerolhcl, hclmethanolic, methanolicchoh, chohesters, estersreaction, reactioncorn, cornacid, acidextra, extramethyl, methylbyproducts, byproductsincomplete, incompletedmso
TheReporterReprinted from Volume 16, No. 3, 1997T297053© 1999 Sigma-Aldrich Co.For more information, or current prices, contact your nearest Supelco subsidiary listed below. To obtain further contact information, visit our website (www.sigma-aldrich.com), see the Supelco catalog, orcontact Supelco, Bellefonte, PA 16823-0048...
Klíčová slova
transesterification, transesterificationglycerol, glycerolhcl, hcllipid, lipidesters, esterscorn, cornreaction, reactionmethanolic, methanolictriglyceride, triglyceridefatty, fattybyproducts, byproductsdmso, dmsoacid, acidoil, oilexcess
Bulletin 909AGuide to Derivatization Reagents for GCA large number of reagents are used to prepare derivatives forgas chromatography, but most of the derivatization reactionsfit into one of three categories: acylation, alkylation, orsilylation. This bulletin describes each category, and presentsinformation on...
Klíčová slova
trimethylsilyl, trimethylsilylethers, etherstmcs, tmcstmsi, tmsibstfa, bstfaalkylation, alkylationsilylation, silylationhmds, hmdsesters, estersacylation, acylationdmf, dmfsupelco, supelcobsa, bsadialkylacetals, dialkylacetalsreagents
Bulletin 909AGuide to Derivatization Reagents for GCA large number of reagents are used to prepare derivatives forgas chromatography, but most of the derivatization reactionsfit into one of three categories: acylation, alkylation, orsilylation. This bulletin describes each category, and presentsinformation on...
Klíčová slova
trimethylsilyl, trimethylsilylethers, etherstmcs, tmcstmsi, tmsibstfa, bstfaalkylation, alkylationsilylation, silylationhmds, hmdsesters, estersacylation, acylationdmf, dmfsupelco, supelcobsa, bsadialkylacetals, dialkylacetalsreagents
 

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