Pressure-Balanced Headspace for the Determination of Class I, II and III Residual Solvents in Pharmaceuticals by USP Chapter <467> Methodology | LabRulez GCMS
 

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A P P L I C AT I O N N O T EGas ChromatographyAuthor:David ScottPerkinElmer, Inc.Shelton, CTResidual Solvents inPharmaceuticals by USPChapter <467> MethodologyIntroductionThe synthesis of activepharmaceutical ingredients(API) may require multiplereaction steps that produceundesirable reaction byproducts or utilize various solvents...
Klíčová slova
headspace, headspacesolvents, solventsresidual, residualpressure, pressurevial, vialintegration, integrationwithdraw, withdrawsampler, samplerscott, scottreaction, reactionrequire, requireexperimental, experimentalpermissible, permissibleturbomatrix, turbomatrixbalanced
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoBulletin 933Capillary GC Column Choices for Residual Solvent AnalysesUsing Direct Injection or Solid Phase Microextraction* (SPME)There is a variety of solvents used in pharmaceutical processing. In the...
Klíčová slova
dipole, dipolespme, spmesupelco, supelcoacetate, acetateresidual, residualsolvents, solventsretention, retentionheadspace, headspaceidentification, identificationmin, minbutanol, butanoltime, timeimmersion, immersionxylene, xylenebutyl
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoBulletin 933Capillary GC Column Choices for Residual Solvent AnalysesUsing Direct Injection or Solid Phase Microextraction* (SPME)There is a variety of solvents used in pharmaceutical processing. In the...
Klíčová slova
dipole, dipolespme, spmesupelco, supelcoacetate, acetateresidual, residualsolvents, solventsretention, retentionheadspace, headspaceidentification, identificationmin, minbutanol, butanoltime, timeimmersion, immersionxylene, xylenebutyl
Capillary GC ColumnChoices for ResidualSolvent AnalysesUsing Direct Injection orSolid Phase Microextraction(SPME)The life science businessof Merck operates asMilliporeSigma in theU.S. and Canada. In the process of preparing a pharmaceutical product, you can potentially retain residualorganic solvents in the final preparation. In the...
Klíčová slova
dipole, dipolespme, spmefiber, fiberacetate, acetateresidual, residualretention, retentioncolumn, columnheadspace, headspacechoices, choicesanalytes, analytesidentification, identificationtime, timebutanol, butanolsolvents, solventsimmersion
 

Podobná PDF

Toggle
A P P L I C AT I O N N O T EGas ChromatographyAuthor:David ScottPerkinElmer, Inc.Shelton, CTResidual Solvents inPharmaceuticals by USPChapter <467> MethodologyIntroductionThe synthesis of activepharmaceutical ingredients(API) may require multiplereaction steps that produceundesirable reaction byproducts or utilize various solvents...
Klíčová slova
headspace, headspacesolvents, solventsresidual, residualpressure, pressurevial, vialintegration, integrationwithdraw, withdrawsampler, samplerscott, scottreaction, reactionrequire, requireexperimental, experimentalpermissible, permissibleturbomatrix, turbomatrixbalanced
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoBulletin 933Capillary GC Column Choices for Residual Solvent AnalysesUsing Direct Injection or Solid Phase Microextraction* (SPME)There is a variety of solvents used in pharmaceutical processing. In the...
Klíčová slova
dipole, dipolespme, spmesupelco, supelcoacetate, acetateresidual, residualsolvents, solventsretention, retentionheadspace, headspaceidentification, identificationmin, minbutanol, butanoltime, timeimmersion, immersionxylene, xylenebutyl
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoBulletin 933Capillary GC Column Choices for Residual Solvent AnalysesUsing Direct Injection or Solid Phase Microextraction* (SPME)There is a variety of solvents used in pharmaceutical processing. In the...
Klíčová slova
dipole, dipolespme, spmesupelco, supelcoacetate, acetateresidual, residualsolvents, solventsretention, retentionheadspace, headspaceidentification, identificationmin, minbutanol, butanoltime, timeimmersion, immersionxylene, xylenebutyl
Capillary GC ColumnChoices for ResidualSolvent AnalysesUsing Direct Injection orSolid Phase Microextraction(SPME)The life science businessof Merck operates asMilliporeSigma in theU.S. and Canada. In the process of preparing a pharmaceutical product, you can potentially retain residualorganic solvents in the final preparation. In the...
Klíčová slova
dipole, dipolespme, spmefiber, fiberacetate, acetateresidual, residualretention, retentioncolumn, columnheadspace, headspacechoices, choicesanalytes, analytesidentification, identificationtime, timebutanol, butanolsolvents, solventsimmersion
 

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