Cannabidiol Oil Analysis with the Pyroprobe | LabRulez GCMS
 

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#198Quantitative Cannabidiol Oil Analysis with the PyroprobeApplication NotePharmaceutical -CannabisAbstractThis application note demonstrates quantitative analysis of CBD oil includingAuthor:RSDs and a calibration curve.Karen SamA previously published application note1 describes Cannabidiol (CBD) oil qualitatively examined using a multi-step temperature sequence2,3. This article...
Klíčová slova
pyroprobe, pyroprobecannabidiol, cannabidiolquantitative, quantitativeadept, adeptkaren, karencounts, countsoil, oilcapsules, capsulesmedication, medicationsolving, solvingsam, samcbd, cbdtenax, tenaxcannabis, cannabisequation
Streamlining Cannabis Testing Using Comprehensive Two-Dimensional Gas Chromatographywith Time-of-Flight Mass Spectrometry (GCxGC-TOFMS)Brad Barrett, David E. Alonso, and Joe Binkley | LECO Corporation, St. Joseph, MI USABackground•••The composition of cannabis is very important in determining its utility, potency,and medicinal effectivenessCannabis is...
Klíčová slova
tofms, tofmsmarijauana, marijauanagcxgc, gcxgccamphorene, camphoreneamyrin, amyrincannabis, cannabiscbd, cbdmass, massisocaryophyllene, isocaryophyllenemyrtenal, myrtenalsimilarity, similaritybenzenemethanol, benzenemethanolfamesene, famesenerecreation, recreationbromofos
Streamlining Cannabis Testing Using GC-MS and GCxGC-MSDavid E. Alonso and Joe Binkley | LECO Corporation, St. Joseph, Michigan 49085BackgroundGC-TOFMS Results: TerpenesC10H16C10H16C10H16C10H164100.009524334484630.000.000.00925954865δ 3-careneD-Limonene1,8-CineoleC10H16C10H16C10H18O4704874910.000.000.00922966879β-Ocimeneγ-Terpinene3,8-p-MenthadieneL-FenchoneC10H16C10H16C10H16C10H16O5035165450.000.000.009708357585470.00795Linalool1,3,8-p-MenthatrieneFencholPinanolcis-p-Mentha-2,8-dien-1-olIpsdienolC10H18OC10H14C10H18OC10H18OC10H16OC10H16O5525675700.010.000.009418149645795885950.000.060.00885797889(+)-2-BornanonePinocarvoneendo-BorneolTerpinen-4-olC10H16OC10H14OC10H18OC10H18O6016176206290.010.000.000.00850813963895α-TerpineolC10H18O6400.01943Formula R.T. (s) M ∆ (Da) SimilarityC10H14O6540.007736600.00896C10H14O6900.07814C10H18O7720.00805C10H14ONamePerillalVerbenoneGeraniol3-Terpinolenoneα-CubebeneYlangeneCopaeneβ-Guaieneβ-Yalangeneβ-CubebeneSelina-5,11-dieneCadineneSantaleneIsocaryophylleneα-GuaieneAromandendrene(E)-β-FameseneHumuleneAlloaromadendreneγ-Muuroleneα-Selineneβ-Bisaboleneγ-Cadineneδ-CadineneFormulaC15H22(E)-α-Bisaboleneα-CalacoreneCaryophyllene oxideGuaiol(-)-GlobulolHumulene epoxide 2Selin-6-en-4α-ol(-)-10-epiγ-EudsemolAristolene(-)-α-PanasinsenC15H24C15H20C15H24OC15H26OC15H26OC15H24OC15H26OC15H26OC15H24C15H247767968000.000.000.00909926904C15H24C15H248050.007808080.00749C15H24C15H24C15H268108178280.000.00-0.02798884893C15H248320.00866C15H24C15H24C15H24C15H248378488528540.000.000.009608259300.02884C15H24C15H24C15H248648698780.000.000.00955959855C15H24C15H248950.00943α-BisabololLedeneJunipercamphorAromadendrane-4,10-diolIsoaromadendrene epoxideSpathulanolCorymbolonem-Camphorenep-CamphorenePhytol8970.00966NeophytadieneC15H24C15H249079120.000.00932892R.T. (s) M ∆ (Da) Similarity9130.008619219290.000.009468789619669759799859870.000.000.000.000.010.00936935918868814928100210120.00-0.24756767C15H26OC15H24C15H26OC15H26O2C15H24OC15H26OC15H24O2C20H32C20H32C20H40O102210291038110111271144116911880.010.000.010.010.000.000.000.01922855853824789751794851120812740.010.02818951C20H382120-0.02887Ave.: |Mass Δ|=0.01, Similarity...
Klíčová slova
calacorene, calacorenetofms, tofmsgcxgc, gcxgcmyrtenal, myrtenalcamphorene, camphorenecannabis, cannabisname, namecadinene, cadinenetrue, trueguaiene, guaieneacid, acidcubebene, cubebenebisabolene, bisabolenemarijuana, marijuanaaic
Cannabis Testing SolutionsTerpene Analysis by HS-GCMSDr. Manuel BraunShimadzu Europa GmbH Terpenes• Terpenes – organic, fragrant compounds produced by plants• Distinctive flavor and aroma• Primary constitute of essential oils of medical plants• Medicinal hydrocarbon building blocks• Terpenes in cannabis• Terpenes are produced...
Klíčová slova
terpene, terpeneterpenes, terpenesgcms, gcmspinene, pinenecannabis, cannabiscaryophyllene, caryophyllenecrushing, crushingcannabinoids, cannabinoidslimonene, limonenesynergistic, synergisticeffect, effectcannabisbud, cannabisbudheadspacer, headspacereucalyptol, eucalyptolprofiling
 

Podobná PDF

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#198Quantitative Cannabidiol Oil Analysis with the PyroprobeApplication NotePharmaceutical -CannabisAbstractThis application note demonstrates quantitative analysis of CBD oil includingAuthor:RSDs and a calibration curve.Karen SamA previously published application note1 describes Cannabidiol (CBD) oil qualitatively examined using a multi-step temperature sequence2,3. This article...
Klíčová slova
pyroprobe, pyroprobecannabidiol, cannabidiolquantitative, quantitativeadept, adeptkaren, karencounts, countsoil, oilcapsules, capsulesmedication, medicationsolving, solvingsam, samcbd, cbdtenax, tenaxcannabis, cannabisequation
Streamlining Cannabis Testing Using Comprehensive Two-Dimensional Gas Chromatographywith Time-of-Flight Mass Spectrometry (GCxGC-TOFMS)Brad Barrett, David E. Alonso, and Joe Binkley | LECO Corporation, St. Joseph, MI USABackground•••The composition of cannabis is very important in determining its utility, potency,and medicinal effectivenessCannabis is...
Klíčová slova
tofms, tofmsmarijauana, marijauanagcxgc, gcxgccamphorene, camphoreneamyrin, amyrincannabis, cannabiscbd, cbdmass, massisocaryophyllene, isocaryophyllenemyrtenal, myrtenalsimilarity, similaritybenzenemethanol, benzenemethanolfamesene, famesenerecreation, recreationbromofos
Streamlining Cannabis Testing Using GC-MS and GCxGC-MSDavid E. Alonso and Joe Binkley | LECO Corporation, St. Joseph, Michigan 49085BackgroundGC-TOFMS Results: TerpenesC10H16C10H16C10H16C10H164100.009524334484630.000.000.00925954865δ 3-careneD-Limonene1,8-CineoleC10H16C10H16C10H18O4704874910.000.000.00922966879β-Ocimeneγ-Terpinene3,8-p-MenthadieneL-FenchoneC10H16C10H16C10H16C10H16O5035165450.000.000.009708357585470.00795Linalool1,3,8-p-MenthatrieneFencholPinanolcis-p-Mentha-2,8-dien-1-olIpsdienolC10H18OC10H14C10H18OC10H18OC10H16OC10H16O5525675700.010.000.009418149645795885950.000.060.00885797889(+)-2-BornanonePinocarvoneendo-BorneolTerpinen-4-olC10H16OC10H14OC10H18OC10H18O6016176206290.010.000.000.00850813963895α-TerpineolC10H18O6400.01943Formula R.T. (s) M ∆ (Da) SimilarityC10H14O6540.007736600.00896C10H14O6900.07814C10H18O7720.00805C10H14ONamePerillalVerbenoneGeraniol3-Terpinolenoneα-CubebeneYlangeneCopaeneβ-Guaieneβ-Yalangeneβ-CubebeneSelina-5,11-dieneCadineneSantaleneIsocaryophylleneα-GuaieneAromandendrene(E)-β-FameseneHumuleneAlloaromadendreneγ-Muuroleneα-Selineneβ-Bisaboleneγ-Cadineneδ-CadineneFormulaC15H22(E)-α-Bisaboleneα-CalacoreneCaryophyllene oxideGuaiol(-)-GlobulolHumulene epoxide 2Selin-6-en-4α-ol(-)-10-epiγ-EudsemolAristolene(-)-α-PanasinsenC15H24C15H20C15H24OC15H26OC15H26OC15H24OC15H26OC15H26OC15H24C15H247767968000.000.000.00909926904C15H24C15H248050.007808080.00749C15H24C15H24C15H268108178280.000.00-0.02798884893C15H248320.00866C15H24C15H24C15H24C15H248378488528540.000.000.009608259300.02884C15H24C15H24C15H248648698780.000.000.00955959855C15H24C15H248950.00943α-BisabololLedeneJunipercamphorAromadendrane-4,10-diolIsoaromadendrene epoxideSpathulanolCorymbolonem-Camphorenep-CamphorenePhytol8970.00966NeophytadieneC15H24C15H249079120.000.00932892R.T. (s) M ∆ (Da) Similarity9130.008619219290.000.009468789619669759799859870.000.000.000.000.010.00936935918868814928100210120.00-0.24756767C15H26OC15H24C15H26OC15H26O2C15H24OC15H26OC15H24O2C20H32C20H32C20H40O102210291038110111271144116911880.010.000.010.010.000.000.000.01922855853824789751794851120812740.010.02818951C20H382120-0.02887Ave.: |Mass Δ|=0.01, Similarity...
Klíčová slova
calacorene, calacorenetofms, tofmsgcxgc, gcxgcmyrtenal, myrtenalcamphorene, camphorenecannabis, cannabisname, namecadinene, cadinenetrue, trueguaiene, guaieneacid, acidcubebene, cubebenebisabolene, bisabolenemarijuana, marijuanaaic
Cannabis Testing SolutionsTerpene Analysis by HS-GCMSDr. Manuel BraunShimadzu Europa GmbH Terpenes• Terpenes – organic, fragrant compounds produced by plants• Distinctive flavor and aroma• Primary constitute of essential oils of medical plants• Medicinal hydrocarbon building blocks• Terpenes in cannabis• Terpenes are produced...
Klíčová slova
terpene, terpeneterpenes, terpenesgcms, gcmspinene, pinenecannabis, cannabiscaryophyllene, caryophyllenecrushing, crushingcannabinoids, cannabinoidslimonene, limonenesynergistic, synergisticeffect, effectcannabisbud, cannabisbudheadspacer, headspacereucalyptol, eucalyptolprofiling
 

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