16 Priority PAHs and Methylnaphthalenes on Rxi- 5Sil MS using the GC Accelerator Kit in a 208 V Oven | LabRulez GCMS

16 Priority PAHs and Methylnaphthalenes on Rxi- 5Sil MS using the GC Accelerator Kit in a 208 V OvenAplikace | | Restek Instrumentace
GC/MSD, GC/SQ, GC kolony, Spotřební materiál
Zaměření
Životní prostředí
Výrobce
Agilent Technologies, Restek
Klíčová slova

 

Podobná PDF

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Featured Application: Fast PAH Analysis at Low Levels Using the GC Accelerator KitIncrease Sample Throughput with New 15-Minute, Low-LevelPAH GC-MS Analysis• Scaled-down column and method open the door to faster PAH analysis; the GC Accelerator kit boosts oven ramp rates...
Klíčová slova
revised, revisedaccelerator, acceleratorbenzo, benzomix, mixdescription, descriptionkit, kitsurrogate, surrogatefluoranthene, fluoranthenescaled, scaledpah, pahanthracene, anthracenepyrene, pyrenefluoranthenes, fluoranthenesoven, ovensame
Select PAHs on Rxi®-PAH (60 m x 0.25 mm x 0.10 µm)1,27 PeakstR (min)1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.6.176.217.087.327.978.129.399.659.7710.4211.616.8117.5617.7618.0722.9322.9329.6432.8237.7546.1446.3849.1349.6449.7349.9650.1556.2463.86Naphthalene-D8Naphthalene2-Methylnaphthalene1-MethylnaphthaleneBiphenyl2,6-DimethylnaphthaleneAcenaphthyleneAcenaphthene-D10Acenaphthene2,3,5-TrimethylnaphthaleneFluoreneDibenzothiophenePhenanthrene-D10PhenanthreneAnthracene4H-Cyclopenta[def]phenanthrene1-MethylphenanthreneFluoranthenePyreneBenzo[c]fluoreneBenzo[ghi]fluorantheneBenzo[c]phenanthreneBenz[a]anthraceneCyclopenta[cd]pyreneChrysene-D12TriphenyleneChrysene5-MethylchryseneBenzo[b]fluorantheneConc. Quant Ion Peaks(µg/mL)2.012830. Benzo[k]fluoranthene9.313631. Benzo[j]fluoranthene2.514232. Benzo[a]fluoranthene2.514233. Benzo[e]pyrene4.915434. Benzo[a]pyrene-D122.515635. Benzo[a]pyrene7.116236. Perylene-D122.015237. Perylene6.815338. Dibenzo[a,j]anthracene2.517039. Dibenzo[a,c]anthracene6.416540. Indeno[1,2,3-cd]pyrene4.418441. Dibenzo[a,h]anthracene2.018842. Benzo[b]chrysene9.417843. Picene6.017844. Benzo[ghi]perylene1.019045. Anthanthrene2.519246. Dibenzo[b,k]fluoranthene8.020247. Dibenzo[a,l]pyrene8.220248. Dibenzo[a,e]pyrene2.521649. Coronene-D121.522650. Coronene2.022851. Dibenzo[a,i]pyrene8.822852. Dibenzo[a,h]pyrene5.22262.02401.82288.92284.424210252tR (min)64.1364.2965.1067.1567.3867.6368.3868.6274.4675.1875.3175.3976.1176.4577.0877.8782.2382.5184.1884.3684.5185.1585.6641441454093529111815634 848232616,17Diluent:Conc.:InjectionInj....
Klíčová slova
benzo, benzofluoranthene, fluoranthenefluorene, fluorenephenanthrene, phenanthreneanthracene, anthracenepyrene, pyrenemin, mincyclopenta, cyclopentadibenzothiophene, dibenzothiophenetriphenylene, triphenylenepeaks, peaksghi, ghiextractor, extractorbenz, benzbiphenyl
16 Priority PAHs and Methylnaphthalenes on Rxi-5Sil MS using the GC Accelerator Kit in a 120 V Oven18,19111,2Ion 276.10Ion 278.10Ion 138.0015,16175121367 832014BenzoFluoranthenesValley= 71.58% 2410.58 min9421 2223262725103.504.004.505.005.506.006.507.00Time (min)7.508.008.509.009.5010.0010.50GC_EV1472 1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.PeaksNaphthalene-d8 (IS)Naphthalene2-Methylnaphthalene1-Methylnaphthalene2-Fluorobiphenyl (SS)AcenaphthyleneAcenaphthene-d10 (IS)AcenaphtheneFluorene2,4,6-Tribromophenol (SS)Phenanthrene-d10 (IS)PhenanthreneAnthraceneFluoranthenePyrene-d10 (SS)Pyrenep-Terphenyl-D14 (SS)Benz[a]anthraceneChrysene-d12 (IS)ChryseneBenzo[b]fluorantheneBenzo[k]fluorantheneBenzo[a]pyrenePerylene-d12 (IS)Indeno[1,2,3-cd]pyreneDibenz[a,h]anthraceneBenzo[ghi]perylenetR (min)3.443.453.863.924.084.414.494.514.834.975.405.415.456.156.286.296.377.127.137.158.178.218.568.6410.1610.2010.58Conc. (µg/mL)2.01.01.01.02.01.02.01.01.02.02.01.01.01.02.01.02.01.02.01.01.01.01.02.01.01.01.0© 2017 Restek...
Klíčová slova
benzo, benzofluoranthene, fluorantheneanthracene, anthracenepyrene, pyrenefluoranthenes, fluoranthenesdftpp, dftppmin, minghi, ghiextractor, extractorperylene, perylenebenz, benzacenaphthylene, acenaphthyleneacenaphthene, acenaphthenefluorene, fluorenephenanthrene
Semivolatiles on Rxi-5Sil MS by U.S. EPA Method 8270 Using the GC Accelerator Kit and Split Injection witha 208 V GC OvenBAIon 184.00Ion 162.00CTF= 0.96Ion 93Valley= 84.58%7051,5235 4036413130411,1224,2517,18,1929 3210145,6331572823 27132120982216155D768678727381464542564767643938384,85Ion 276.00Ion 278.00TIC Valley= 46.40%4844377163583479,807469501,4-Dioxane-87759,60,61Ion 252.00Valley= 76.56%6690 9187539493925749 544375898883826568622621.40 1.60 1.80...
Klíčová slova
phthalate, phthalatebenzo, benzofluoranthene, fluoranthenebenzyl, benzyldiphenylhydrazine, diphenylhydrazineanthracene, anthracenepyrene, pyrenepeaks, peaksbutyl, butylmin, minnitrosodi, nitrosodinitrosodiphenylamine, nitrosodiphenylaminedftpp, dftppcarbazole, carbazoleazobenzene

16 Priority PAHs and Methylnaphthalenes on Rxi- 5Sil MS using the GC Accelerator Kit in a 208 V OvenAplikace | | Restek Instrumentace
GC/MSD, GC/SQ, GC kolony, Spotřební materiál
Zaměření
Životní prostředí
Výrobce
Agilent Technologies, Restek
Klíčová slova

 

Podobná PDF

Toggle
Featured Application: Fast PAH Analysis at Low Levels Using the GC Accelerator KitIncrease Sample Throughput with New 15-Minute, Low-LevelPAH GC-MS Analysis• Scaled-down column and method open the door to faster PAH analysis; the GC Accelerator kit boosts oven ramp rates...
Klíčová slova
revised, revisedaccelerator, acceleratorbenzo, benzomix, mixdescription, descriptionkit, kitsurrogate, surrogatefluoranthene, fluoranthenescaled, scaledpah, pahanthracene, anthracenepyrene, pyrenefluoranthenes, fluoranthenesoven, ovensame
Select PAHs on Rxi®-PAH (60 m x 0.25 mm x 0.10 µm)1,27 PeakstR (min)1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.6.176.217.087.327.978.129.399.659.7710.4211.616.8117.5617.7618.0722.9322.9329.6432.8237.7546.1446.3849.1349.6449.7349.9650.1556.2463.86Naphthalene-D8Naphthalene2-Methylnaphthalene1-MethylnaphthaleneBiphenyl2,6-DimethylnaphthaleneAcenaphthyleneAcenaphthene-D10Acenaphthene2,3,5-TrimethylnaphthaleneFluoreneDibenzothiophenePhenanthrene-D10PhenanthreneAnthracene4H-Cyclopenta[def]phenanthrene1-MethylphenanthreneFluoranthenePyreneBenzo[c]fluoreneBenzo[ghi]fluorantheneBenzo[c]phenanthreneBenz[a]anthraceneCyclopenta[cd]pyreneChrysene-D12TriphenyleneChrysene5-MethylchryseneBenzo[b]fluorantheneConc. Quant Ion Peaks(µg/mL)2.012830. Benzo[k]fluoranthene9.313631. Benzo[j]fluoranthene2.514232. Benzo[a]fluoranthene2.514233. Benzo[e]pyrene4.915434. Benzo[a]pyrene-D122.515635. Benzo[a]pyrene7.116236. Perylene-D122.015237. Perylene6.815338. Dibenzo[a,j]anthracene2.517039. Dibenzo[a,c]anthracene6.416540. Indeno[1,2,3-cd]pyrene4.418441. Dibenzo[a,h]anthracene2.018842. Benzo[b]chrysene9.417843. Picene6.017844. Benzo[ghi]perylene1.019045. Anthanthrene2.519246. Dibenzo[b,k]fluoranthene8.020247. Dibenzo[a,l]pyrene8.220248. Dibenzo[a,e]pyrene2.521649. Coronene-D121.522650. Coronene2.022851. Dibenzo[a,i]pyrene8.822852. Dibenzo[a,h]pyrene5.22262.02401.82288.92284.424210252tR (min)64.1364.2965.1067.1567.3867.6368.3868.6274.4675.1875.3175.3976.1176.4577.0877.8782.2382.5184.1884.3684.5185.1585.6641441454093529111815634 848232616,17Diluent:Conc.:InjectionInj....
Klíčová slova
benzo, benzofluoranthene, fluoranthenefluorene, fluorenephenanthrene, phenanthreneanthracene, anthracenepyrene, pyrenemin, mincyclopenta, cyclopentadibenzothiophene, dibenzothiophenetriphenylene, triphenylenepeaks, peaksghi, ghiextractor, extractorbenz, benzbiphenyl
16 Priority PAHs and Methylnaphthalenes on Rxi-5Sil MS using the GC Accelerator Kit in a 120 V Oven18,19111,2Ion 276.10Ion 278.10Ion 138.0015,16175121367 832014BenzoFluoranthenesValley= 71.58% 2410.58 min9421 2223262725103.504.004.505.005.506.006.507.00Time (min)7.508.008.509.009.5010.0010.50GC_EV1472 1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.PeaksNaphthalene-d8 (IS)Naphthalene2-Methylnaphthalene1-Methylnaphthalene2-Fluorobiphenyl (SS)AcenaphthyleneAcenaphthene-d10 (IS)AcenaphtheneFluorene2,4,6-Tribromophenol (SS)Phenanthrene-d10 (IS)PhenanthreneAnthraceneFluoranthenePyrene-d10 (SS)Pyrenep-Terphenyl-D14 (SS)Benz[a]anthraceneChrysene-d12 (IS)ChryseneBenzo[b]fluorantheneBenzo[k]fluorantheneBenzo[a]pyrenePerylene-d12 (IS)Indeno[1,2,3-cd]pyreneDibenz[a,h]anthraceneBenzo[ghi]perylenetR (min)3.443.453.863.924.084.414.494.514.834.975.405.415.456.156.286.296.377.127.137.158.178.218.568.6410.1610.2010.58Conc. (µg/mL)2.01.01.01.02.01.02.01.01.02.02.01.01.01.02.01.02.01.02.01.01.01.01.02.01.01.01.0© 2017 Restek...
Klíčová slova
benzo, benzofluoranthene, fluorantheneanthracene, anthracenepyrene, pyrenefluoranthenes, fluoranthenesdftpp, dftppmin, minghi, ghiextractor, extractorperylene, perylenebenz, benzacenaphthylene, acenaphthyleneacenaphthene, acenaphthenefluorene, fluorenephenanthrene
Semivolatiles on Rxi-5Sil MS by U.S. EPA Method 8270 Using the GC Accelerator Kit and Split Injection witha 208 V GC OvenBAIon 184.00Ion 162.00CTF= 0.96Ion 93Valley= 84.58%7051,5235 4036413130411,1224,2517,18,1929 3210145,6331572823 27132120982216155D768678727381464542564767643938384,85Ion 276.00Ion 278.00TIC Valley= 46.40%4844377163583479,807469501,4-Dioxane-87759,60,61Ion 252.00Valley= 76.56%6690 9187539493925749 544375898883826568622621.40 1.60 1.80...
Klíčová slova
phthalate, phthalatebenzo, benzofluoranthene, fluoranthenebenzyl, benzyldiphenylhydrazine, diphenylhydrazineanthracene, anthracenepyrene, pyrenepeaks, peaksbutyl, butylmin, minnitrosodi, nitrosodinitrosodiphenylamine, nitrosodiphenylaminedftpp, dftppcarbazole, carbazoleazobenzene
 

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