Determining Terpene Profiles of Cannabis Strains Using GC and GCxGC with High Performance TOFMS | LabRulez GCMS
 

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®Fast Analysis of Citronella Ceylon Oilwith GC-TOFMSLECO Corporation; Saint Joseph, Michigan USAKey Words: GC-TOFMS1. IntroductionThere are two types of citronella oil - ceylon and java both of which are valued for their lemony aromas. Ceylonis the more common variety and...
Klíčová slova
geranyl, geranyltrans, transcis, ciscadinene, cadineneocimene, ocimenebutyrate, butyrateoxide, oxideelemol, elemolacetate, acetateelemicin, elemicincadinol, cadinolcitronellyl, citronellylspectra, spectrapegasus, pegasusisoeugenol
Streamlining Cannabis Testing Using Comprehensive Two-Dimensional Gas Chromatographywith Time-of-Flight Mass Spectrometry (GCxGC-TOFMS)Brad Barrett, David E. Alonso, and Joe Binkley | LECO Corporation, St. Joseph, MI USABackground•••The composition of cannabis is very important in determining its utility, potency,and medicinal effectivenessCannabis is...
Klíčová slova
tofms, tofmsmarijauana, marijauanagcxgc, gcxgccamphorene, camphoreneamyrin, amyrincannabis, cannabiscbd, cbdmass, massisocaryophyllene, isocaryophyllenemyrtenal, myrtenalsimilarity, similaritybenzenemethanol, benzenemethanolfamesene, famesenerecreation, recreationbromofos
Fingerprinting the Terpene Profiles of Various Cannabis Strains using GC and GCxGC with High Performance TOFMSDavid E. Alonso1, Julie Kowalski2, and Joseph E. Binkley1 | 1LECO Corporation, St. Joseph, Michigan; 2Trace Analytics, Spokane, WashingtonGCxGC-TOFMS Cannabis Analysis: Representative CompoundsData Acquisition &...
Klíčová slova
camphorene, camphorenesimilarity, similaritycannabis, cannabiscalacorene, calacorenefenchone, fenchoneformula, formuladendrasaline, dendrasalinelimona, limonaterpene, terpenecorymbolone, corymbolonetofms, tofmstrue, trueterpenes, terpenescalamenene, calamenenename
Streamlining Cannabis Testing Using GC-MS and GCxGC-MSDavid E. Alonso and Joe Binkley | LECO Corporation, St. Joseph, Michigan 49085BackgroundGC-TOFMS Results: TerpenesC10H16C10H16C10H16C10H164100.009524334484630.000.000.00925954865δ 3-careneD-Limonene1,8-CineoleC10H16C10H16C10H18O4704874910.000.000.00922966879β-Ocimeneγ-Terpinene3,8-p-MenthadieneL-FenchoneC10H16C10H16C10H16C10H16O5035165450.000.000.009708357585470.00795Linalool1,3,8-p-MenthatrieneFencholPinanolcis-p-Mentha-2,8-dien-1-olIpsdienolC10H18OC10H14C10H18OC10H18OC10H16OC10H16O5525675700.010.000.009418149645795885950.000.060.00885797889(+)-2-BornanonePinocarvoneendo-BorneolTerpinen-4-olC10H16OC10H14OC10H18OC10H18O6016176206290.010.000.000.00850813963895α-TerpineolC10H18O6400.01943Formula R.T. (s) M ∆ (Da) SimilarityC10H14O6540.007736600.00896C10H14O6900.07814C10H18O7720.00805C10H14ONamePerillalVerbenoneGeraniol3-Terpinolenoneα-CubebeneYlangeneCopaeneβ-Guaieneβ-Yalangeneβ-CubebeneSelina-5,11-dieneCadineneSantaleneIsocaryophylleneα-GuaieneAromandendrene(E)-β-FameseneHumuleneAlloaromadendreneγ-Muuroleneα-Selineneβ-Bisaboleneγ-Cadineneδ-CadineneFormulaC15H22(E)-α-Bisaboleneα-CalacoreneCaryophyllene oxideGuaiol(-)-GlobulolHumulene epoxide 2Selin-6-en-4α-ol(-)-10-epiγ-EudsemolAristolene(-)-α-PanasinsenC15H24C15H20C15H24OC15H26OC15H26OC15H24OC15H26OC15H26OC15H24C15H247767968000.000.000.00909926904C15H24C15H248050.007808080.00749C15H24C15H24C15H268108178280.000.00-0.02798884893C15H248320.00866C15H24C15H24C15H24C15H248378488528540.000.000.009608259300.02884C15H24C15H24C15H248648698780.000.000.00955959855C15H24C15H248950.00943α-BisabololLedeneJunipercamphorAromadendrane-4,10-diolIsoaromadendrene epoxideSpathulanolCorymbolonem-Camphorenep-CamphorenePhytol8970.00966NeophytadieneC15H24C15H249079120.000.00932892R.T. (s) M ∆ (Da) Similarity9130.008619219290.000.009468789619669759799859870.000.000.000.000.010.00936935918868814928100210120.00-0.24756767C15H26OC15H24C15H26OC15H26O2C15H24OC15H26OC15H24O2C20H32C20H32C20H40O102210291038110111271144116911880.010.000.010.010.000.000.000.01922855853824789751794851120812740.010.02818951C20H382120-0.02887Ave.: |Mass Δ|=0.01, Similarity...
Klíčová slova
calacorene, calacorenetofms, tofmsgcxgc, gcxgcmyrtenal, myrtenalcamphorene, camphorenecannabis, cannabisname, namecadinene, cadinenetrue, trueguaiene, guaieneacid, acidcubebene, cubebenebisabolene, bisabolenemarijuana, marijuanaaic
 

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®Fast Analysis of Citronella Ceylon Oilwith GC-TOFMSLECO Corporation; Saint Joseph, Michigan USAKey Words: GC-TOFMS1. IntroductionThere are two types of citronella oil - ceylon and java both of which are valued for their lemony aromas. Ceylonis the more common variety and...
Klíčová slova
geranyl, geranyltrans, transcis, ciscadinene, cadineneocimene, ocimenebutyrate, butyrateoxide, oxideelemol, elemolacetate, acetateelemicin, elemicincadinol, cadinolcitronellyl, citronellylspectra, spectrapegasus, pegasusisoeugenol
Streamlining Cannabis Testing Using Comprehensive Two-Dimensional Gas Chromatographywith Time-of-Flight Mass Spectrometry (GCxGC-TOFMS)Brad Barrett, David E. Alonso, and Joe Binkley | LECO Corporation, St. Joseph, MI USABackground•••The composition of cannabis is very important in determining its utility, potency,and medicinal effectivenessCannabis is...
Klíčová slova
tofms, tofmsmarijauana, marijauanagcxgc, gcxgccamphorene, camphoreneamyrin, amyrincannabis, cannabiscbd, cbdmass, massisocaryophyllene, isocaryophyllenemyrtenal, myrtenalsimilarity, similaritybenzenemethanol, benzenemethanolfamesene, famesenerecreation, recreationbromofos
Fingerprinting the Terpene Profiles of Various Cannabis Strains using GC and GCxGC with High Performance TOFMSDavid E. Alonso1, Julie Kowalski2, and Joseph E. Binkley1 | 1LECO Corporation, St. Joseph, Michigan; 2Trace Analytics, Spokane, WashingtonGCxGC-TOFMS Cannabis Analysis: Representative CompoundsData Acquisition &...
Klíčová slova
camphorene, camphorenesimilarity, similaritycannabis, cannabiscalacorene, calacorenefenchone, fenchoneformula, formuladendrasaline, dendrasalinelimona, limonaterpene, terpenecorymbolone, corymbolonetofms, tofmstrue, trueterpenes, terpenescalamenene, calamenenename
Streamlining Cannabis Testing Using GC-MS and GCxGC-MSDavid E. Alonso and Joe Binkley | LECO Corporation, St. Joseph, Michigan 49085BackgroundGC-TOFMS Results: TerpenesC10H16C10H16C10H16C10H164100.009524334484630.000.000.00925954865δ 3-careneD-Limonene1,8-CineoleC10H16C10H16C10H18O4704874910.000.000.00922966879β-Ocimeneγ-Terpinene3,8-p-MenthadieneL-FenchoneC10H16C10H16C10H16C10H16O5035165450.000.000.009708357585470.00795Linalool1,3,8-p-MenthatrieneFencholPinanolcis-p-Mentha-2,8-dien-1-olIpsdienolC10H18OC10H14C10H18OC10H18OC10H16OC10H16O5525675700.010.000.009418149645795885950.000.060.00885797889(+)-2-BornanonePinocarvoneendo-BorneolTerpinen-4-olC10H16OC10H14OC10H18OC10H18O6016176206290.010.000.000.00850813963895α-TerpineolC10H18O6400.01943Formula R.T. (s) M ∆ (Da) SimilarityC10H14O6540.007736600.00896C10H14O6900.07814C10H18O7720.00805C10H14ONamePerillalVerbenoneGeraniol3-Terpinolenoneα-CubebeneYlangeneCopaeneβ-Guaieneβ-Yalangeneβ-CubebeneSelina-5,11-dieneCadineneSantaleneIsocaryophylleneα-GuaieneAromandendrene(E)-β-FameseneHumuleneAlloaromadendreneγ-Muuroleneα-Selineneβ-Bisaboleneγ-Cadineneδ-CadineneFormulaC15H22(E)-α-Bisaboleneα-CalacoreneCaryophyllene oxideGuaiol(-)-GlobulolHumulene epoxide 2Selin-6-en-4α-ol(-)-10-epiγ-EudsemolAristolene(-)-α-PanasinsenC15H24C15H20C15H24OC15H26OC15H26OC15H24OC15H26OC15H26OC15H24C15H247767968000.000.000.00909926904C15H24C15H248050.007808080.00749C15H24C15H24C15H268108178280.000.00-0.02798884893C15H248320.00866C15H24C15H24C15H24C15H248378488528540.000.000.009608259300.02884C15H24C15H24C15H248648698780.000.000.00955959855C15H24C15H248950.00943α-BisabololLedeneJunipercamphorAromadendrane-4,10-diolIsoaromadendrene epoxideSpathulanolCorymbolonem-Camphorenep-CamphorenePhytol8970.00966NeophytadieneC15H24C15H249079120.000.00932892R.T. (s) M ∆ (Da) Similarity9130.008619219290.000.009468789619669759799859870.000.000.000.000.010.00936935918868814928100210120.00-0.24756767C15H26OC15H24C15H26OC15H26O2C15H24OC15H26OC15H24O2C20H32C20H32C20H40O102210291038110111271144116911880.010.000.010.010.000.000.000.01922855853824789751794851120812740.010.02818951C20H382120-0.02887Ave.: |Mass Δ|=0.01, Similarity...
Klíčová slova
calacorene, calacorenetofms, tofmsgcxgc, gcxgcmyrtenal, myrtenalcamphorene, camphorenecannabis, cannabisname, namecadinene, cadinenetrue, trueguaiene, guaieneacid, acidcubebene, cubebenebisabolene, bisabolenemarijuana, marijuanaaic
 

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